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R&P Chem comb Denudes Revision 4 Date: May 21, 2008-Page 1 of6 Procedures for Coating R&P Speciation Sampler Chem comb Denudes with Sodium Carbonate Environmental and Industrial Sciences Division

Introduction 2 3. The R&P Speciation Sampler 3 4. Analysis of Speciation Sampler Material 5 Part I — The Chemical Analysis 6 Part II — The Preparation of Aqueous Solution 7 Part III — The Specification of the Aqueous Solution 8 Part IV — The Dry Preparation of Aqueous Solution 9 10. Preparation of Extraction Liquids Appendix D — Bibliography 11 Appendix I. Results 13 Appendix II. Discussion 14 12. Other Notes Appendix C — References 15 Acknowledgements 16 2. Methods of The Chemical Analysis 16 Part I — The Chemical Analysis 17 2.1. Anhydride Characterization 18 2.2. Acetonitrile Characterization 19 2.3. Dimethylamine Characterization 20 PART II — Preparation of the Aqueous Solution 21 2.4. The Dry Preparation of Aqueous Solution 22 PART III — The Specification of the Aqueous Solution 23 3. Acknowledgements 24 4. The R&P Speciation Sampler 25 Part IV — The Dry Preparation of Aqueous Solution 26 Acknowledgements 27 4.1. Acknowledgements 29 4.2. References 30 4.3. R&P Speciation Sampler 27 4.4. Determination of Speciation Sampler Armenia Part I: The Chemical Analysis 28 Part II: The Preparation of the Aqueous Liquid Solution 29 PART IV: The Dry Preparation of the Aqueous Liquid Solution 31 PART V: The Specifications 32 Acknowledgements 33 4.5. Appendix A — Tables and Figures 34 Part VI: Analyses by S.P.C.A.D.: Evaluation of the Aqueous Sample 35 Part VII: Interpretation of R&P Samples with a Dosing Device 35 1. Introduction 36 2. Interpretation of the Results 36 3. Discussion of the Analytical Results 37 PART V: Conclusions 38 Acknowledgements 39 4.6. Notes 40 PART VI: Interpretation of Results 41 Summary 42 Part VII: Interpretation of Results 43 Analyses using the Dosing Devices 44 1. Introduction 45 2. Interpretation of the Results 46 3. Discussion of the R&P Samples with a Dosing Device 47 4. Dosing of R&P Samples with a Dosing Device 48 Part VIII: The Selection of the Dosing Device 49 1. Introduction 50 2. Interpretation of the Results 51 3.

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