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NOVEL CATALYST FOR THE REMOVAL OF AROMATIC SULFUR SPECIES FROM REFINERY STREAMS By Franz Georg Retold B.S., University of Louisville, 2010 A Thesis Submitted to the Faculty of the University of Louisville

H. J. Pickering, Department of Chemical Engineering September 14, 2010 The purpose of this work is to improve the quality of Sulfur-bearing products, such as fuel oil as well as petroleum feedstocks, especially by producing an all-carbon synthetic catalyst which yields high energy per gram catalyst, a high yield and a high purity. In the conventional Sulfur-containing reagents, such as peroxide and per oxygen, the sulfurous species are highly abundant owing to the large numbers present in nature. It can be easily detected. The process of a catalyst can only be conducted on a large scale with a high efficiency. In order to obtain an extremely high catalytic efficiency one has to obtain a high catalyst material concentration. The development and selection of a suitable catalyst material are a major area of research. It represents a major hurdle in the practical application of such synthetic systems. Several alternative high-synthetic-product and high-efficiency synthetic catalysts have been investigated that can be obtained by a number of mechanisms. The synthesis of such materials is still a large research field. The synthesis of a high-synthesis-efficiency catalyst is an active area of experimental research for practical application in fuel oil production. The main objective of this project would be to synthesize a new supersonic superoxide anion oxidizer in a pure sulfuric acid, a new supersonic superoxide hetero-oxide hydrogenation fuel-oil catalyst. In doing so, we would be able to realize a new process that has the potential to lower CO 2 emissions and to increase the energy efficiency of the fuel product. Synthesis The primary catalyst material to be used for this project is peroxynitrate. When the reactivity of peroxynitrate is increased, the reactions occur more frequently and efficiently. This enhances the performance of the reaction. The reaction is conducted on an anode with a copper cathode. A copper layer is deposited on the outside of the cathode and the cathode are an aqueous solution of peroxide and per oxygen. In a second reaction, one would also place a layer of gold to improve the reaction temperature. A layer of nickel would be placed on the second anode cathode after the reaction to maintain a high surface area for efficient reaction with oxygen. In order to achieve the maximum possible reactivity, an ion exchange is done with two electrodes immersed in the solution.

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