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Lawrence Berkeley National Laboratory Lawrence Berkeley National Laboratory Title Selective oxidation of methanol and ethanol on supported ruthenium oxide clusters at low temperaturesPermalink https://escholarship.org/uc/item/42j639f0Authors Liu,

How to fill out selective oxidation of methanol

How to fill out selective oxidation of methanol

1. Step 1: Prepare the reactants. You will need methanol, an oxidizing agent such as air or oxygen, and a catalyst.
2. Step 2: Set up the reaction vessel. This can be a suitable glass or stainless steel container with a lid and the necessary connections for gas flow and temperature control.
3. Step 3: Add the catalyst to the reaction vessel. Common catalysts for selective oxidation of methanol include copper, silver, or metal oxides like manganese oxide.
4. Step 4: Introduce the methanol into the reaction vessel. This can be done using a syringe or a controlled pump.
5. Step 5: Supply the oxidizing agent. If using air, you can introduce it by bubbling air through the reaction mixture. If using oxygen, it can be supplied through a separate inlet.
6. Step 6: Control the reaction conditions. Maintain a suitable temperature and pressure to promote the selective oxidation of methanol. This can vary depending on the catalyst used.
7. Step 7: Allow the reaction to proceed for the desired duration. This can range from minutes to hours, depending on the extent of oxidation desired.
8. Step 8: Monitor the progress of the reaction. This can be done through periodic sampling and analysis of the reaction mixture using techniques such as gas chromatography.
9. Step 9: Once the desired level of oxidation is achieved, stop the reaction by removing the supply of methanol and the oxidizing agent.
10. Step 10: Purify the oxidation product. This may involve filtration, distillation, or other separation techniques to isolate the desired product from any unreacted starting materials or by-products.
11. Step 11: Characterize and analyze the purified product to confirm its identity and purity.
12. Step 12: Dispose of the reaction waste safely and responsibly, following applicable regulations.

Who needs selective oxidation of methanol?

1. The selective oxidation of methanol is commonly used in the chemical industry for the production of various valuable chemicals such as formaldehyde, acetic acid, and formaldehyde derivatives.
2. It is also of interest in academic research for studying the catalytic properties of different catalysts and exploring new reaction pathways.
3. Furthermore, selective oxidation of methanol holds potential for environmental applications, such as the removal of volatile organic compounds (VOCs) from air or the conversion of methanol into more environmentally friendly fuels.

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