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J. Am. Chem. SOC.1987, 109, 4642-4648 4642 with a 14.305 A, b 12.995 A, c 14.595 A, phi 93.16O, V 2709 A, and Z 8. A total of 4165 reflections were recorded on a Philips PW 1100 diffractometer in
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