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NMR Spectroscopy Sample Submission Form
Chem NMR Spectroscopy Facility
University of North Carolina at Greensboro
301 Cover Street
005 Sullivan Science Building
Greensboro, NC 27412
3362568608 (lab)
http://www.uncg.edu/cheFranklin
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How to fill out nmr spectroscopy sample submission
How to fill out nmr spectroscopy sample submission
01
Obtain a sample of the substance that you want to analyze using NMR spectroscopy. This can be a liquid or solid sample.
02
Prepare the sample by dissolving it in a suitable solvent. The choice of solvent depends on the nature of the sample and the type of NMR analysis you require.
03
Ensure that the concentration of the sample is appropriate for NMR analysis. Typically, a concentration of 1-10 mg/mL is used for liquid samples.
04
Transfer the prepared sample into a suitable NMR tube. The NMR tube should be clean and free from any contaminants.
05
Label the NMR tube with the necessary information such as the sample name, concentration, and any other relevant details.
06
Place the labeled NMR tube into the spectrometer for analysis. Follow the specific instructions of the spectrometer to load the sample correctly.
07
Run the NMR experiment according to the desired parameters. This includes setting the desired temperature, pulse sequence, and acquisition parameters.
08
Monitor the NMR spectrum during the experiment to ensure the data quality. Adjust the experiment parameters if necessary.
09
Once the NMR experiment is complete, carefully remove the NMR tube from the spectrometer and clean it properly for reuse or disposal.
10
Analyze the obtained NMR spectrum to interpret the chemical shifts, integration values, and other relevant information about the sample.
Who needs nmr spectroscopy sample submission?
01
NMR spectroscopy sample submission is needed by various professionals and researchers in the fields of chemistry, biochemistry, pharmaceuticals, materials science, and other related disciplines. It is commonly used to determine the structure, composition, and purity of organic and inorganic compounds. Researchers, scientists, and analytical laboratories often require NMR spectroscopy sample submission to analyze and characterize their samples for research, quality control, and identification purposes.
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What is nmr spectroscopy sample submission?
NMR spectroscopy sample submission is the process of submitting samples for analysis using nuclear magnetic resonance spectroscopy.
Who is required to file nmr spectroscopy sample submission?
Researchers, scientists, and individuals conducting NMR spectroscopy experiments are required to file sample submissions.
How to fill out nmr spectroscopy sample submission?
To fill out NMR spectroscopy sample submission, one must provide details about the sample, experiment conditions, and contact information.
What is the purpose of nmr spectroscopy sample submission?
The purpose of NMR spectroscopy sample submission is to analyze the molecular structure and chemical composition of a sample.
What information must be reported on nmr spectroscopy sample submission?
Information such as sample name, solvent used, concentration, NMR parameters, and any special instructions must be reported on the sample submission form.
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