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1Experiment 11: Bromination of Silent
In the experiment entitled Steam Distillation, you demonstrated that eugenol has
one or more carbon double bonds by reacting it with bromine, Br2, and observing
the
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How to fill out bromination of stilbene
01
Start by adding 2 mL of acetone to a 50 mL round-bottom flask.
02
Add a stir bar to the flask and place it on a magnetic stir plate.
03
Weigh out 0.5 g of stilbene and add it to the flask.
04
Slowly add 3 mL of bromine to the flask using a syringe, while stirring continuously.
05
Allow the reaction mixture to stir at room temperature for 30 minutes.
06
After 30 minutes, quench the reaction by adding 10 mL of water to the flask.
07
Extract the organic layer with dichloromethane three times, using 10 mL each time.
08
Dry the organic layer with anhydrous sodium sulfate.
09
Filter the solution to remove any solids or impurities.
10
Concentrate the solution using rotary evaporation.
11
Purify the product using column chromatography or recrystallization.
12
Analyze the purified product using spectroscopy techniques for characterizations.
Who needs bromination of stilbene?
01
The bromination of stilbene is commonly performed by organic chemists as a synthetic method to introduce a bromine group into the stilbene molecule. This reaction can be used for further transformations or to create new compounds with desired properties. Additionally, researchers in various fields may use brominated stilbene derivatives for their specific studies or applications.
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What is bromination of stilbene?
Bromination of stilbene is a chemical reaction where a bromine atom is added to the carbon-carbon double bond of a stilbene molecule.
Who is required to file bromination of stilbene?
Chemical manufacturers or facilities conducting the bromination of stilbene are required to file the necessary documentation.
How to fill out bromination of stilbene?
Bromination of stilbene must be filled out according to the specific guidelines and regulations set by the governing authorities.
What is the purpose of bromination of stilbene?
The purpose of bromination of stilbene is to introduce a bromine atom to the stilbene molecule for further chemical reactions.
What information must be reported on bromination of stilbene?
Information such as the quantity of stilbene used, the method of bromination, safety precautions taken, and disposal methods must be reported.
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