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Point by point steps to fill out structure elucidation in organic:

1. Understand the problem: Before starting the structure elucidation process, it is essential to have clarity on the problem at hand. This involves gathering all relevant information regarding the unknown compound, such as its physical properties, spectroscopic data, and any other available experimental data.
2. Analyze spectroscopic data: The most common techniques used in organic structure elucidation are nuclear magnetic resonance (NMR), infrared spectroscopy (IR), mass spectrometry (MS), and UV-Vis spectroscopy. Analyze the spectra obtained from these techniques to identify characteristic peaks and functional groups present in the compound.
3. Determine the molecular formula: Using the information obtained from the spectroscopic data, calculate the compound's molecular formula. This can be done by comparing the mass spectrometry data with theoretical molecular weights or by considering the number of signals in the NMR spectra.
4. Identify the molecular connectivity: Based on the analysis of the spectra, determine the connectivity of atoms in the molecule. This involves interpreting the NMR coupling patterns, identifying chemical shifts, and considering the splitting patterns of signals in the spectra.
5. Assign functional groups: Apply the obtained spectroscopic information to assign functional groups to the molecule. This can be done by matching characteristic peaks in the IR spectra with known functional group vibrations.
6. Verify the structure: Once the molecular connectivity and functional groups have been assigned, verify the proposed structure by comparing it with the experimental data. This includes comparing the calculated and observed spectra and ensuring they are in agreement.

Who needs structure elucidation in organic?

1. Chemists: Organic chemists use structure elucidation techniques to identify unknown compounds, verify synthesized compounds, or characterize organic materials.
2. Pharmaceutical industry: Structure elucidation is crucial in the pharmaceutical industry for drug discovery and development. It helps in identifying new compounds, determining their structures, and understanding their interactions.
3. Forensic investigators: Structure elucidation plays a vital role in forensic investigations. It helps in identifying illicit substances, analyzing unknown compounds found at crime scenes, and providing evidence for legal cases.
4. Environmental scientists: Structure elucidation techniques are used in environmental science to identify and analyze organic pollutants, such as pesticides and industrial contaminants, in air, water, and soil samples.
5. Natural product researchers: Structure elucidation is essential in natural product research to identify and characterize bioactive compounds present in plants, microorganisms, and marine organisms.

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