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CHEM 108LUCSC, BinderExperiment 1: Recrystallization of Acetanilide Reading Assignment Morris 2 4 (Glassware, Reagents, & Heating) & 14 15 (Melting Point & Recrystallization) The purification of organic
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How to fill out exp 1 - recrystallization

01
Start by weighing the sample of the compound you want to recrystallize.
02
Dissolve the compound in a suitable solvent. The choice of solvent will depend on the compound and its solubility.
03
Heat the solvent and compound mixture gently to aid dissolution.
04
Once the compound is completely dissolved, remove any insoluble impurities by filtration.
05
Slowly cool the solution to allow the compound to crystallize. This can be done by placing the solution in an ice bath or by leaving it at room temperature.
06
Collect the crystals by filtration and wash them with a small amount of cold solvent to remove any remaining impurities.
07
Dry the crystals thoroughly, either by air drying or using a desiccator.
08
Weigh the purified crystals to determine the yield and assess the success of the recrystallization process.

Who needs exp 1 - recrystallization?

01
Exp 1 - recrystallization is commonly used by chemists and researchers working with organic compounds.
02
It is used to purify a compound, removing impurities such as other organic compounds, inorganic salts, or residual solvents.
03
The recrystallization technique helps in obtaining a higher purity of the compound, which is essential for accurate characterization and further use in various applications.
04
It is particularly useful for isolating and purifying solid organic compounds from a mixture, or for removing impurities from a solid sample.
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exp 1 - recrystallization is a process used in chemistry to purify a solid compound by dissolving it in a solvent and then allowing it to slowly crystallize.
Researchers and scientists conducting experiments in the field of chemistry are required to file exp 1 - recrystallization.
To fill out exp 1 - recrystallization, one must document the procedure followed during the recrystallization process, the compounds used, any observations made, and the results obtained.
The purpose of exp 1 - recrystallization is to obtain a pure sample of a compound by removing impurities through the process of crystallization.
The information that must be reported on exp 1 - recrystallization includes the starting material, the solvent used, the method of recrystallization, any impurities detected, and the yield obtained.
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