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Rapid GC Simulated Distillation Analysis Max Wang, Clifford M. Taylor, Shimizu Scientific Instruments; Steve MacDonald, Zip Scientific GC-2010 Simulated Distillation Gas Chromatography Racer Abstract:
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The new SIDES Method is based on the same basic concept. ASTM D 2797, Gas Chromatograph Separation and Identification by Carbon Dioxide (H 2 CO 3) and Chlorine Dioxide (Halo), describes a gas chromatographic method that identifies volatile substances with an ion chromatographic peak (1-4). The gas chromatographic method that was developed at the University of California, Los Angeles is now available in the form of the Sides Method. During the analysis performed in this method, volatile substances that were previously masked by the addition of sulfur trioxide are observed by the GC. ASTM D 2772, Gas chromatographic separation in pure gas chromatography systems (GC-HPLC) — a method for separating gas chromatography fractions according to their mass ranges for analytical analysis — was published by the Institute of Chemistry of the Chinese Academy of Sciences in January 1995. The method was designed for the chromatographic separation of ethyl alcohol and ethanol in a gas chromatographic column. The Sides Method is used to determine the volatile substances remaining in the sample and this enables the separation of both ethyl alcohol and other alcohols in a gas chromatographic column as well as alcohol compounds present in the sample. The methods for the Sides Method were developed by Professor Clifford M. Taylor, Director of the Center for Compound Analysis and Engineering, and Professors Steve MacDonald and Clifford M. Taylor. The analytical methods used in this method are not related to the gas chromatographic separation methods described in ASTM D 2887, ASTM D 2871, ASTM D 2872 and ASTM D 2695. This method is specifically designed for GC-HPLC. The Sides Method can be used for gas chromatographic separation of compounds, such as compounds of alcohol, as well as compounds, such as ethyl alcohol, that may be derived from these compounds. In this method, a volatile substance, such as ethyl alcohol, is placed in a sealed compartment. A sample is then placed in the sample compartment and separated against the column by mixing the column with the sample mixture. The separation of ethyl alcohol was determined by measuring the peak position of a benzene derivative in the separation column and the separation of other alkenes.

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