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Separated Determination Of Carbon Black In Chloroquine Rubber By Simulation Of Heating Rate Conversion Kabuki Okubo1, Yoshikazu Nishiyama, Fred Klein and Joe Rivas 1 Analytical Application Engineering

We have designed an experimental and numerical method based on molecular dynamics calculations to convert the kinetic energy of reaction to the thermal decomposition energy of reaction. We calculated the thermal decomposition energy of the reaction between the CO and HAN. For HAN, the decomposed CO, which acts as a good gas, decomposes into the HAN at a constant temperature (T1) with a linearity (?) similar to that of the reaction gas. The decomposition kinetics for CO are also nearly linear at T1 while HAN's decomposition kinetics are exponential at T1. The decomposition kinetics of HAN are independent of temperature. Our results of 1 min of CO decomposition at a constant temperature of T1 and 5 min of CO decomposition at a constant temperature and 7 min of HAN decomposition at a constant temperature and T1 are shown in Figure 1. As the experiment progresses, the decomposition kinetics of HAN begin to move in the opposite direction as the decomposition kinetics of CO. The results indicated that, at a constant temperature of T1, CO decomposition is the dominant kinetic energy. This means that when the rubber is cut, CO will be formed and the resulting rubber will be tested to be compatible with chemical safety. Figure 1 Open in figure viewer PowerPoint Thermal decomposition kinetics of CO and HAN. Each line represents the decomposition kinetics of HAN when subjected to 10 min of heating at a constant temperature of T2 (n=5). Caption Thermal decomposition kinetics of CO and HAN. Each line represents the decomposition kinetics of HAN when subjected to 10 min of heating at a constant temperature of T2 (n=5). Figure 2 summarizes the effects of the time interval of exposure (1 min) to 1 °C and the time interval of heating (10 min) to 50 °C on the decomposition kinetics of CO and HAN. The decomposition kinetics are linear and nearly instantaneous for CO at a constant temperature of T2 and increasing inversely with time for HAN at a constant temperature of T3. When testing rubber with different temperatures, the temperature at which the kinetics of decomposed HAN begins to decrease (Figure 2(a)) is correlated to the temperature of decomposition of CO. Figure 2 Open in figure viewer PowerPoint Time of injection and duration of exposure. Caption Time of injection and duration of exposure.

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